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Organic Chemistry I laboratory

Undergraduate · Chemistry

Syllabus focus

Standard syllabus · STEM / applied

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$1,162 · Organic Chemistry I laboratory · 18 tutoring hrs

Study guides, worksheets, reviews, practice tests, and answer keys for 1 class. 18 tutoring hours (1 hr / week · semester). Bundle discount applied vs buying separately. Pay in full via Zelle or Venmo.

Topics typically covered

Standard syllabus

Organic lab safety and notebook culture

  • Flammables, corrosives, and peroxide-forming solvents
  • Fume hood practice and waste segregation for organics
  • Carbon-copy or ELN notebook expectations
  • Tracking theoretical yield, actual yield, and percent yield
  • Pre-lab questions tied to mechanism and hazards

Core purification techniques

  • Recrystallization and melting-point purity checks
  • Simple and fractional distillation
  • Extraction and drying of organic layers
  • Rotary evaporation and solvent removal
  • Choosing a purification method from impurity profile

Chromatography

  • TLC for reaction monitoring and identity checks
  • Column chromatography basics
  • Rf interpretation and co-spotting
  • Solvent polarity and elution order
  • Isolating a product fraction and assessing purity

Synthesis labs (Orgo I scope)

  • Substitution and elimination product studies (as scheduled)
  • Alkene addition or related first-semester transformations
  • Workup logic: quench, extract, dry, concentrate
  • Stereochemistry observations where experiments allow
  • Connecting mechanism lectures to observed outcomes

Structure evidence (intro spectroscopy)

  • IR functional-group identification of products
  • Melting point / mixed melting point for identity
  • Intro ¹H NMR sample prep and simple assignments
  • Reporting spectral evidence in lab reports
  • Troubleshooting failed reactions with TLC/IR clues

Green and microscale practice

  • Microscale apparatus and yield discipline
  • Solvent choice and waste minimization
  • Atom economy discussion for a course synthesis
  • Safe scale-down of a published procedure
  • Reflection: technique mastery vs one-off recipes

STEM / applied

Applied organic skills

  • Multi-period synthesis with intermediate characterization
  • Literature procedure adaptation for available reagents
  • Formal organic lab report (ACS-style sections)
  • Technique checklist for research-lab readiness
  • Oral technique demo or notebook audit

Notes

Companion lab to Organic Chemistry I lecture. Focuses on technique and purification that make Orgo II multistep work possible.